4-(4-Nitro­benzene­sulfonamido)pyridinium trifluoro­acetate

نویسندگان

  • Jiang-Sheng Li
  • Mei-Lian Fan
  • Wen-Sheng Li
  • Wei-Dong Liu
چکیده

In the title compound, C(11)H(10)N(3)O(4)S(+)·C(2)F(3)O(2) (-), the benzene ring makes an angle of 87.3 (2)° with the pyridinium ring. The nitro group is essentially coplanar with the benzene ring. The F atoms of the CF(3) group are disordered over two positions with almost equal occupancy [0.531 (12)/0.469 (12)]. The crystal structure is stabilized by N-H⋯O and C-H⋯O hydrogen bonds.

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منابع مشابه

4-(2-Nitro­benzene­sulfonamido)pyri­dinium trifluoro­acetate

In the title compound, C(11)H(10)N(3)O(4)S(+)·C(2)F(3)O(2) (-), the dihedral angle between the benzene ring and the pyridinium ring is 88.7 (4)°. In the crystal structure, a network of N-H⋯O, C-H⋯O and C-H⋯F hydrogen bonds links the constituent ions. One O atom of the nitro group is disordered over two positions, with site-occupancy factors of 0.57 (2) and 0.43 (2).

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4-(4-Nitro­benzene­sulfonamido)pyridinium bromide

In the title compound, C(11)H(10)N(3)O(4)S(+)·Br(-), the benzene ring makes an angle of 88.4 (2)° with the pyridinium ring. The dihedral angle between the nitro group and the benzene ring is 16.5 (2)°. The ions in the crystal structure are linked by a combination of inter-molecular N-H⋯Br and non-conventional C-H⋯Br and C-H⋯O hydrogen bonds, forming a three-dimensional network.

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4-(4-Nitro­benzene­sulfonamido)pyridinium trichloro­acetate

In the title compound, C(11)H(10)N(3)O(4)S(+)·C(2)Cl(3)O(2) (-), the benzene ring forms an angle of 85.21 (13)° with the pyridinium ring. The nitro group is nearly coplanar with its attached benzene ring [dihedral angle = 3.68 (12)°]. In the crystal structure, strong N-H⋯O hydrogen bonds link the ion-pairs. The packing is further consolidated by weak C-H⋯O inter-ations.

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4-(4-Nitro­benzene­sulfonamido)pyridinium nitrate

A short C-N distance [1.394 (2) Å] in the title compound, C(11)H(10)N(3)O(4)S(+)·NO(3) (-), is indicative of some conjugation of the sulfonamide π electrons with those of the pyridinium ring. The crystal structure is stabilized by N-H⋯O hydrogen bonds.

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4-(2-Nitro­benzene­sulfonamido)pyridinium nitrate

There are two mol-ecules in the asymmetric unit of the title compound, C(11)H(10)N(3)O(4)S(+)·NO(3) (-). All bond distances have normal values. The C-N bond distances in the sulfonamide group [1.389 (3) and 1.382 (3) Å] may indicate slight conjugation of the sulfonamide N-atom π-electrons with those of the pyridinium ring. The crystal structure is stabilized by N-H⋯O hydrogen bonds.

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عنوان ژورنال:

دوره 64  شماره 

صفحات  -

تاریخ انتشار 2008